Wednesday, April 3, 2019

Re-Crystallization of Boric Acid

Re-Crystallization of Boric AcidThe purpose to conduct this lab is recrystallization of whole and then identify the effect on solids purity and yield. small-arm A ReactionsTable 1. quantitative and soft observations of reactions to form boric unpleasant.Mass of borax (g)10.0558g carriage of borax vacuous powderTime for solvability of borax (min)5minTime for boric acid crystals to form (min)12minPart B FiltrationTable 2. kitty of go steady codswallop and filter paper, mass of watch glass, filter paper and wet crystals from filtration and qualitative observations of crystals later on filtration.Mass of watch glass1 an filter paper1(g)33.3364gMass of wet crystals, watch glass 1,filter paper from filtration(g)44.6083gAppearance of crystals subsequently filtrationSoft, white solid formation.Part C Re-crystallizationTable 3. mass of watch glass and filter paper, mass of watch glass, filter paper ad wet crystals from recrystallization, and qualitative observations of crystals afte rward recrystallizationMass of watch glass2 and filter paper2(g)25.2834gMass of watch glass2 ,filter paper2 and recrystallization (g)28.0524gAppearance of crystals after recrystallizationWhite shiny crystal in solid.Part D honesty testTable 4. qualitative observations for the purity test of crystals collected after filtration and recrystallizationObservations of test tube 1, containing crystals after filtration, upon reacting with AgNO3Observations of test tube 2, containing crystals after recrystallization, upon reacting with AgNO3White precipitates formed cl ar present , AgCl formed.Solution is clear, Cl are not present.Table 5. mass of watch glass, filter paper and crystals, and qualitative observations of crystals, after recrystallization and drying.Mass of watch glass 2 + filter paper2+ alter crystals from recrystallization (g)27.4848gAppearance of crystalsWhite solid formation ,shining in bearing . auspicate the wet mass of crystals after the filtration and the recrystalli zation, and dry mass of crystals after the recrystallization. take up your results on ONE table (you should have 3 masses enter in this table)Write the balanced chemical equation for the reaction to pose boric acid. Determine which reactants the limiting reagent. Show all of your work.Calculate the supposed yield of boric acid. show all your work.Calculate the yield of boric acid based on the dry mass of the crystals.Calculate the solubility of boric acid in the water at 250C and 800C using the equations of the best-fit curves that are found in figure 3-2.Explain Why water was an enamor solvent to use for recrystallization in this lab.Explain the differences observed in the appearance of the crystals after filtration compared to the crystals after recrystallizationa) Explain how the purity test is used in this lab to come up the purity of the harvest-tide ( include a balanced chemical equation in your answer).b) based on your observations, are the crystals that you collected followers recrystallization pure? Explain your answer.Other than performing the purity test that was performed in this experiment, develop two other methods that can be used to determine the purity of a product.Discuss the percent yield result. Fully explain two reasons (sources of error) for the loss of product during the experiment, including the specific step at which product was lost. Also explain how each of the losses can be minimized.If you recrystallized the crystals again, what would you foretell to happen? Explain your answer.If during crystallization the solute fails to crystallize, what can be done to include the crystals to form? Explain two ways to induce crystal formation.

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